Introduction to LC-NMR Historical Review Flow and NMR Setting Up the LC-NMR System Solvent Requirements in LC-NMR Solvent Suppression and Referencing The Deuterium Lock The Solvent-Gradient Ramp Diffusion Shimming Acquisition Parameters Chemical-Shift Tracking Other Considerations Sources of Error Summary References NMR Theory Magnetic Properties of Nuclei Data Acquisition Relaxation of Nuclei The Chemical Shift Spin Coupling Nuclear Overhauser Effect (NOE) Coupling of HPLC with NMR References Separation Methods Modes of Separation General Method Development Strategies Column Packing Types Detector Selection RPC Method Development and Compatibility with NMR Integration of CE and NMR Transitioning from Analytical to Preparative Chromatography General Considerations References NMR Instrumentation and Probe Technologies Instrumentation Configuration The Magnet Room Temperature Flow Probe Microcapillary Probes (Room Temperature) Cryogenically Cooled Probes Probe Coil Geometries Probe Sensitivity Comparison References NMR-Associated Isolation Technologies Stopped Flow Loop Collector Solid-Phase Extraction (SPE) Nonchromatographic Flow NMR Direct-Injection NMR (DI-NMR) Capillary Electrophoresis and NMR References NMR Experiments Solvent Suppression Structure Elucidation Experiments NOE Experiments References Applications Degradation Products Impurities Trace Analysis Analysis of Mixtures Tautomer Kinetics Unstable Products Metabolites CE Isolates Natural Products Proteins/Peptides References Other Specialized-Flow NMR NMR and Parallel Detection Data Processing and Deconvolution of Parallel Data Parallel Probe Construction Microprobes Advancements in Multiple-Coil Probe Design Biological Screening and Flow NMR NMR and Microreactors Signal-to-Noise Ratio (Microcoils) Microprobe Design (Microcoil/Microslot/Microstrip) Future Directions Summary References Glossary Index ection RPC Method Development and Compatibility with NMR Integration of CE and NMR Transitioning from Analytical to Preparative Chromatography General Considerations References NMR Instrumentation and Probe Technologies Instrumentation Configuration The Magnet Room Temperature Flow Probe Microcapillary Probes (Room Temperature) Cryogenically Cooled Probes Probe Coil Geometries Probe Sensitivity Comparison References NMR-Associated Isolation Technologies Stopped Flow Loop Collector Solid-Phase Extraction (SPE) Nonchromatographic Flow NMR Direct-Injection NMR (DI-NMR) Capillary Electrophoresis and NMR References NMR Experiments Solvent Suppression Structure Elucidation Experiments NOE Experiments References Applications Degradation Products Impurities Trace Analysis Analysis of Mixtures Tautomer Kinetics Unstable Products Metabolites CE Isolates Natural Products Proteins/Peptides References Other Specialized-Flow NMR NMR and Parallel Detection Data Processing and Deconvolution of Parallel Data Parallel Probe Construction Microprobes Advancements in Multiple-Coil Probe Design Biological Screening and Flow NMR NMR and Microreactors Signal-to-Noise Ratio (Microcoils) Microprobe Design (Microcoil/Microslot/Microstrip) Future Directions Summary References Glossary Index lt;BR>Structure Elucidation Experiments NOE Experiments References Applications Degradation Products Impurities Trace Analysis Analysis of Mixtures Tautomer Kinetics Unstable Products Metabolites CE Isolates Natural Products Proteins/Peptides References Other Specialized-Flow NMR NMR and Parallel Detection Data Processing and Deconvolution of Parallel Data Parallel Probe Construction Microprobes Advancements in Multiple-Coil Probe Design Biological Screening and Flow NMR NMR and Microreactors Signal-to-Noise Ratio (Microcoils) Microprobe Design (Microcoil/Microslot/Microstrip) Future Directions Summary References Glossary Index > Index.